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Suggested Citation:"Front Matter." National Academies of Sciences, Engineering, and Medicine. 2014. Evaluation of the Moisture Susceptibility of WMA Technologies. Washington, DC: The National Academies Press. doi: 10.17226/22429.
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N A T I O N A L C O O P E R A T I V E H I G H W A Y R E S E A R C H P R O G R A M NCHRP REPORT 763 Evaluation of the Moisture Susceptibility of WMA Technologies Amy Epps Martin Edith Arambula Fan Yin Lorena Garcia Cucalon Arif Chowdhury Robert Lytton Jon Epps Cindy Estakhri Eun Sug Park Texas a&M TransporTaTion insTiTuTe The Texas a&M universiTy sysTeM College Station, TX Subscriber Categories Highways • Materials TRANSPORTAT ION RESEARCH BOARD WASHINGTON, D.C. 2014 www.TRB.org Research sponsored by the American Association of State Highway and Transportation Officials in cooperation with the Federal Highway Administration

NATIONAL COOPERATIVE HIGHWAY RESEARCH PROGRAM Systematic, well-designed research provides the most effective approach to the solution of many problems facing highway administrators and engineers. Often, highway problems are of local interest and can best be studied by highway departments individually or in cooperation with their state universities and others. However, the accelerating growth of highway transportation develops increasingly complex problems of wide interest to highway authorities. These problems are best studied through a coordinated program of cooperative research. In recognition of these needs, the highway administrators of the American Association of State Highway and Transportation Officials initiated in 1962 an objective national highway research program employing modern scientific techniques. This program is supported on a continuing basis by funds from participating member states of the Association and it receives the full cooperation and support of the Federal Highway Administration, United States Department of Transportation. The Transportation Research Board of the National Academies was requested by the Association to administer the research program because of the Board’s recognized objectivity and understanding of modern research practices. The Board is uniquely suited for this purpose as it maintains an extensive committee structure from which authorities on any highway transportation subject may be drawn; it possesses avenues of communications and cooperation with federal, state and local governmental agencies, universities, and industry; its relationship to the National Research Council is an insurance of objectivity; it maintains a full-time research correlation staff of specialists in highway transportation matters to bring the findings of research directly to those who are in a position to use them. The program is developed on the basis of research needs identified by chief administrators of the highway and transportation departments and by committees of AASHTO. Each year, specific areas of research needs to be included in the program are proposed to the National Research Council and the Board by the American Association of State Highway and Transportation Officials. Research projects to fulfill these needs are defined by the Board, and qualified research agencies are selected from those that have submitted proposals. Administration and surveillance of research contracts are the responsibilities of the National Research Council and the Transportation Research Board. The needs for highway research are many, and the National Cooperative Highway Research Program can make significant contributions to the solution of highway transportation problems of mutual concern to many responsible groups. The program, however, is intended to complement rather than to substitute for or duplicate other highway research programs. Published reports of the NATIONAL COOPERATIVE HIGHWAY RESEARCH PROGRAM are available from: Transportation Research Board Business Office 500 Fifth Street, NW Washington, DC 20001 and can be ordered through the Internet at: http://www.national-academies.org/trb/bookstore Printed in the United States of America NCHRP REPORT 763 Project 09-49 ISSN 0077-5614 ISBN 978-0-309-28368-7 Library of Congress Control Number 2013953982 © 2014 National Academy of Sciences. All rights reserved. COPYRIGHT INFORMATION Authors herein are responsible for the authenticity of their materials and for obtaining written permissions from publishers or persons who own the copyright to any previously published or copyrighted material used herein. Cooperative Research Programs (CRP) grants permission to reproduce material in this publication for classroom and not-for-profit purposes. Permission is given with the understanding that none of the material will be used to imply TRB, AASHTO, FAA, FHWA, FMCSA, FTA, or Transit Development Corporation endorsement of a particular product, method, or practice. It is expected that those reproducing the material in this document for educational and not-for-profit uses will give appropriate acknowledgment of the source of any reprinted or reproduced material. For other uses of the material, request permission from CRP. NOTICE The project that is the subject of this report was a part of the National Cooperative Highway Research Program, conducted by the Transportation Research Board with the approval of the Governing Board of the National Research Council. The members of the technical panel selected to monitor this project and to review this report were chosen for their special competencies and with regard for appropriate balance. The report was reviewed by the technical panel and accepted for publication according to procedures established and overseen by the Transportation Research Board and approved by the Governing Board of the National Research Council. The opinions and conclusions expressed or implied in this report are those of the researchers who performed the research and are not necessarily those of the Transportation Research Board, the National Research Council, or the program sponsors. The Transportation Research Board of the National Academies, the National Research Council, and the sponsors of the National Cooperative Highway Research Program do not endorse products or manufacturers. Trade or manufacturers’ names appear herein solely because they are considered essential to the object of the report.

The National Academy of Sciences is a private, nonprofit, self-perpetuating society of distinguished scholars engaged in scientific and engineering research, dedicated to the furtherance of science and technology and to their use for the general welfare. On the authority of the charter granted to it by the Congress in 1863, the Academy has a mandate that requires it to advise the federal government on scientific and technical matters. Dr. Ralph J. Cicerone is president of the National Academy of Sciences. The National Academy of Engineering was established in 1964, under the charter of the National Academy of Sciences, as a parallel organization of outstanding engineers. It is autonomous in its administration and in the selection of its members, sharing with the National Academy of Sciences the responsibility for advising the federal government. The National Academy of Engineering also sponsors engineering programs aimed at meeting national needs, encourages education and research, and recognizes the superior achievements of engineers. Dr. C. D. Mote, Jr., is president of the National Academy of Engineering. The Institute of Medicine was established in 1970 by the National Academy of Sciences to secure the services of eminent members of appropriate professions in the examination of policy matters pertaining to the health of the public. The Institute acts under the responsibility given to the National Academy of Sciences by its congressional charter to be an adviser to the federal government and, on its own initiative, to identify issues of medical care, research, and education. Dr. Harvey V. Fineberg is president of the Institute of Medicine. The National Research Council was organized by the National Academy of Sciences in 1916 to associate the broad community of science and technology with the Academy’s purposes of furthering knowledge and advising the federal government. Functioning in accordance with general policies determined by the Academy, the Council has become the principal operating agency of both the National Academy of Sciences and the National Academy of Engineering in providing services to the government, the public, and the scientific and engineering communities. The Council is administered jointly by both Academies and the Institute of Medicine. Dr. Ralph J. Cicerone and Dr. C. D. Mote, Jr., are chair and vice chair, respectively, of the National Research Council. The Transportation Research Board is one of six major divisions of the National Research Council. The mission of the Transporta- tion Research Board is to provide leadership in transportation innovation and progress through research and information exchange, conducted within a setting that is objective, interdisciplinary, and multimodal. The Board’s varied activities annually engage about 7,000 engineers, scientists, and other transportation researchers and practitioners from the public and private sectors and academia, all of whom contribute their expertise in the public interest. The program is supported by state transportation departments, federal agencies including the component administrations of the U.S. Department of Transportation, and other organizations and individu- als interested in the development of transportation. www.TRB.org www.national-academies.org

C O O P E R A T I V E R E S E A R C H P R O G R A M S AUTHOR ACKNOWLEDGMENTS The research reported herein was performed under NCHRP Project 09-49 by the Texas A&M Transpor- tation Institute, a member of The Texas A&M University System. Dr. Amy Epps Martin, Professor of Civil Engineering at Texas A&M University and Research Engineer with the Texas A&M Transportation Insti- tute, served as the Principal Investigator; Ms. Cindy Estakhri, Senior Research Engineer at the Texas A&M Transportation Institute, served as the co-Principal Investigator. Other authors of this report included Dr. Edith Arambula, Fan Yin, Lorena Garcia Cucalon, Arif Chowdhury, Dr. Robert Lytton, Dr. Jon Epps, and Dr. Eun Sug Park, all of the Texas A&M Transportation Institute. Additional important contributors to this work from the Texas A&M Transportation Institute included Dr. David Newcomb, David Zeig, Rick Canatella, Stephen Walls, Stephen Johnson, Sarah Estakhri, Narain Hariharan, Aishwarya Baranikumar, Michael Blaylock, Joe Canatella, Mark Membreño, and Daniel Furdock. The research team gratefully acknowledges the cooperation and assistance provided by the agencies and contractors where field samples were collected, including the Iowa Department of Transportation and Norris Asphalt Paving Company, the Montana Department of Transportation and Jim Gillman Construc- tion, the Texas Department of Transportation and J.D. Ramming Paving Company, and the New Mexico Department of Transportation and James Hamilton Construction Company. In addition, the partner- ship with the Federal Highway Administration Mobile Asphalt Laboratory and other NCHRP warm mix asphalt projects was integral to this work and is greatly appreciated. CRP STAFF FOR NCHRP REPORT 763 Christopher W. Jenks, Director, Cooperative Research Programs Crawford F. Jencks, Deputy Director, Cooperative Research Programs Edward T. Harrigan, Senior Program Officer Anthony P. Avery, Senior Program Assistant Eileen P. Delaney, Director of Publications Hilary Freer, Senior Editor NCHRP PROJECT 09-49 PANEL Field of Bituminous Materials—Area of Materials and Construction Kim A. Willoughby, Washington State DOT, Olympia, WA (Chair) E. Ray Brown, Auburn, AL Ravi V. Chandran, Connecticut DOT, Rocky Hill, CT Matthew Corrigan, Federal Highway Administration, Washington, DC Dale S. Decker, Dale S. Decker, LLC, Eagle, CO Stacey D. Diefenderfer, Virginia Center for Transportation Innovation and Research, Charlottesville, VA Syed Waqar Haider, Michigan State University, East Lansing, MI James L. Horn, Alaska DOT and Public Facilities, Anchorage, AK Rita B. Leahy, California Asphalt Pavement Association, Sacramento, CA Scott A. Schram, Iowa DOT, Ames, IA Dean C. Weitzel, AMEC Environment & Infrastructure, Inc., Carson City, NV Jack H. Springer, FHWA Liaison Frederick Hejl, TRB Liaison

F O R E W O R D This report presents proposed guidelines for identifying potential moisture susceptibility in warm mix asphalt (WMA) and proposed revisions to the Appendix to AASHTO R 35, “Special Mixture Design Considerations and Methods for WMA” to implement the guide- lines. Thus, the report will be of immediate interest to materials engineers in state highway agencies and the asphalt pavement construction industry. Over the past decade, the use of WMA for asphalt pavement construction has dramatically increased in the United States. WMA is seen as an alternative to hot mix asphalt (HMA), which offers the potential to lower energy demand during production and construction, reduce emissions at the plant and the paver, and increase allowable haul distances. How- ever, questions remain about the long-term performance and durability of WMA pave- ments. One key issue is the moisture susceptibility of WMA pavements. Concerns about WMA moisture susceptibility include the possibility that aggregates will be inadequately dried at lower production temperatures and the fact that several WMA technologies intro- duce additional moisture in the production process. The objectives of NCHRP Project 9-49 were to (1) assess whether WMA technologies adversely affect the moisture susceptibility of asphalt pavements and (2) develop guidelines for identifying and limiting moisture susceptibility in WMA pavements. The research was performed by the Texas A&M Transportation Institute, College Station, Texas. The research was conducted through coordinated laboratory and field experiments that investigated the potential for moisture susceptibility in WMA compared to HMA. Design of the experiments was guided by a survey of the state DOTs and industry on WMA pavement construction and performance. The survey identified no instances of moisture damage to WMA pavements in service through 2010. This negative finding is supported by the results of recently completed NCHRP Project 9-47A, which conducted intensive evaluations of WMA pavements constructed across the United States between 2006 and 2011. Project 9-49 then focused on development of guidelines for WMA mix design and quality control to identify and minimize any possibility of moisture susceptibility. The laboratory experiments evaluated (1) laboratory-conditioning protocols for WMA before moisture- susceptibility testing, (2) the ability of standard test methods to detect moisture suscepti- bility of WMA, and (3) potential differences in WMA moisture susceptibility measured on laboratory-mixed and -compacted specimens; plant-mixed, laboratory-compacted speci- mens; and plant-mixed, field-compacted cores. The guidelines are presented in the form of a workflow of conditioning protocols and standard test methods that first assess the potential moisture susceptibility of a WMA mix design or field mixture and then recommend remedies to minimize such susceptibility. By Edward T. Harrigan Staff Officer Transportation Research Board

Specific test thresholds in the guidelines are based on the results of testing of WMA from field projects in Iowa, Montana, New Mexico, and Texas. This report fully documents the research and includes the following Appendixes: • Appendix A. Laboratory Conditioning Experiment • Appendix B. Moisture Conditioning Experiment • Appendix C. Performance Evolution Experiment • Appendix D. Construction Reports and Performance of Field Projects • Appendix E. Mixture Volumetrics • Appendix F. Proposed Draft Revisions to the Appendix to AASHTO R 35 • Appendix G. Future Work Plan to Evaluate Moisture Susceptibility of HMA and WMA • Appendix H. Statistical Results Appendix F is included herein. Appendixes A—E, G, and H are not provided herein but are available on the TRB website and can be found by searching for NCHRP Report 763.

C O N T E N T S 1 Summary 4 Chapter 1 Background 4 History and Definition 4 Benefits and Issues 5 Project Objectives and Scope 6 Relevant Literature and Survey Results 6 WMA Laboratory Conditioning 6 WMA Moisture Susceptibility 8 WMA Performance Evolution 10 Summary of National Survey and Interviews 16 Chapter 2 Research Approach 16 Field Projects 17 Iowa Field Project 19 Montana Field Project 19 Texas Field Project 20 New Mexico Field Project 20 Summary of Compaction Temperatures Used in the Field Projects 20 Laboratory Tests and Specimen Fabrication 20 Laboratory Tests 23 Specimen Fabrication 24 Experiment Designs 24 WMA Laboratory Conditioning 25 WMA Moisture Susceptibility 28 WMA Performance Evolution 31 Chapter 3 Findings and Applications 31 Mixture Volumetrics 31 WMA Laboratory Conditioning 34 WMA Moisture Susceptibility 34 Moisture Susceptibility 37 Effect of Anti-Stripping Agents 38 Effect of Specimen Type 39 WMA Performance Evolution 41 Phase I 42 Phase II 50 Revisions to Draft AASHTO Standards 51 Chapter 4 Findings, Discussion and Guidelines, and Suggested Research 51 Findings 51 WMA Laboratory Conditioning 51 WMA Moisture Susceptibility

52 WMA Performance Evolution 52 Performance Summary 54 Discussion and Guidelines 56 Suggested Research 60 References and Bibliography 65 Appendices A through E, G, and H F-1 Appendix F Note: Many of the photographs, figures, and tables in this report have been converted from color to grayscale for printing. The electronic version of the report (posted on the Web at www.trb.org) retains the color versions.

A B B R E V I A T I O N S , A C R O N Y M S , A N D I N I T I A L I S M S AADT Annual average daily traffic AFM Atomic force microscopy ANOVA Analysis of variance APA Asphalt pavement analyzer ASTM American Society for Testing and Materials AV Air voids BBS Bitumen Bond Strength DSR Dynamic shear rheometer ESAL Equivalent single axle loads FM Farm-to-market F/T Freeze-thaw FT Film thickness HMA Hot mix asphalt HSD Honestly Significant Differences HWTT Hamburg Wheel-Tracking Test IDT Indirect tensile LAS Liquid anti-stripping LCR Remaining life LEA Low emission/energy asphalt LMLC Laboratory-mixed laboratory-compacted LTOA Long-term oven aging LTPP Long-term pavement performance LVDT Linear variable differential transducers MIST Moisture-Induced Stress Tester NAPA National Asphalt Paving Association NCAT National Center for Asphalt Technology PG Performance grade PHT Pavement Health Track PMFC Plant-mixed field-compacted PMLC Plant-mixed plant-compacted QA Quality assurance QC Quality control RAP Reclaimed asphalt pavement RAS Recycled asphalt shingles RDT Repeated direct tension RSL Remaining Service Life SFE Surface Free Energy

SGC Superpave gyratory compactor SIP Stripping inflection point SMA Stone matrix asphalt SN Stripping number STOA Short-term oven aging TSR Tensile strength ratio TWG Technical Working Group TxDOT Texas Department of Transportation WMA Warm mix asphalt

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TRB’s National Cooperative Highway Research Program (NCHRP) Report 763: Evaluation of the Moisture Susceptibility of WMA Technologies presents proposed guidelines for identifying potential moisture susceptibility in warm mix asphalt (WMA). The report also suggests potential revisions to the Appendix to AASHTO R 35, “Special Mixture Design Considerations and Methods for WMA” as a means to implement the guidelines.

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